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Bismuth vanadate synthesized by solution combustion with different fuels: synthesis, characterization and study of photocatalytic activity

机译:用不同燃料的固溶燃烧合成钒酸铋:合成,表征和光催化活性的研究

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摘要

In this manuscript, a BiVO4 semiconductor was synthesized by solution combustion synthesis using different fuels (Alanine, Glycine and Urea). Also, the Tween® 80 surfactant was added during synthesis. BiVO4 was characterized by XRD, SEM and diffuse reflectance spectroscopy. Photocatalytic activity was evaluated by the discoloration of methylene blue at 664 nm under UV-visible light irradiation. According to XRD, the monoclinic phase of BiVO4 was obtained for the samples. The smallest particle size and highest k obs value were observed for the BiVO4/alanine sample, which promoted greater demethylation of methylene blue.
机译:在此手稿中,使用不同的燃料(丙氨酸,甘氨酸和尿素)通过固溶燃烧合成法合成了BiVO4半导体。同样,在合成过程中添加了吐温80表面活性剂。通过XRD,SEM和漫反射光谱对BiVO4进行了表征。通过在UV-可见光照射下在664nm处亚甲基蓝的变色来评价光催化活性。根据XRD,样品获得了BiVO4的单斜晶相。对于BiVO4 /丙氨酸样品,观察到最小的粒径和最高的kobs值,这促进了亚甲基蓝的更大的去甲基化。

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